Name: Thermal Analysis System DSC 5+
Brand: Mettler Toledo

Watch the video and discover the new standard in differential scanning calorimetry.

More Experiments, in a Shorter Time, with Less Resources

Measuring and evaluating samples is a time-consuming task, and it's difficult to ensure consistent interpretation and repeatable results when multiple operators are involved.

To tackle this challenge, DSC 5+ offers you a fully automated solution to simplify sample processing, interpretation, and result assessment, saving valuable time and effort.

‍High Sample Throughput with Advanced Hardware and Software Solutions

The gas-controlled crucible chamber holds 96 sample and 7 reference crucibles for continuous measurement

Let the DSC 5+ Sample Robot Take the Effort Out of Your Work

Enjoy continuous measurement with automated exchange of up to 96 samples and 7 reference crucibles.

Prepare your samples in advance on removable crucible trays. The sample robot automatically detects the tray number and sample position, and applies the correct method.

The universal gripper handles all crucibles ranging from 20 to 160 μL.

Protect your samples before measurement by purging the crucible chamber with an inert gas, such as nitrogen.

To prevent contamination of fresh samples and free up space on the crucible tray, the robot can automatically drop the used crucibles in the crucible bin.

Unique System of Robot Lid Piercing and Removal For Sensitive Samples

Removable lid to protect sensitive samples
Hermetical sealing of crucibles
Precisely defined hole made by the robot in the lid
No contact with the sample
No change in sample mass during the wait cycle

Protect Even the Most Sensitive Samples

For sensitive samples the crucible can be hermetically sealed to prevent any changes in sample mass before the measurement starts.

Just before the measurement begins, DSC 5+ robot's built-in needle pierces the special crucible lid making a precisely defined hole without coming into the contact with the sample.

Sensitive samples can also be protected with a special removable lid.

The robot removes the lid just before the measurement starts.

After the measurement, the robot puts the lid back on the crucible and returns it to the tray.

Brochure: DSC 5+ Differential Scanning Calorimeter

Download the DSC 5+ Brochure

The METTLER TOLEDO DSC 5+ redefines performance. The innovative MMS 1 sensor features 136 thermocouples as well as 2 integrated heaters for power compensation mode. This enables extremely accurate measurement of both weak and close-lying effects. The 96-position sample robot boosts productivity and ensures safe crucible handling without operator intervention.

Download the brochure to see how you can perform more experiments, in a shorter time, with fewer resources.

Unique Power Compensation Mode

Outstanding Resolution for the Separation of Close-Lying Effects

How Does Power Compensation Mode Work in the DSC 5+?

For the first time, a single furnace DSC can measure with power compensation.

Two integrated heaters in the state-of-the-art MMS 1 sensor keep the temperature difference (ΔT) between the sample and reference as close to zero as possible. During a measurement, any enthalpy change in the sample is compensated by the appropriate heater so that ΔT = 0.

The amount of heat power introduced to compensate for any enthalpy change is very precisely measured, leading to a heat flow signal with outstanding resolution.

Watch the short video above to see the sensor heaters in action!

What Are the Benefits of Power Compensation Mode in the DSC 5+?

In power compensation mode, the very short signal-time constant provides excellent resolution and the ability to separate close-lying thermal effects.

Together with the star-shaped arrangement of 136 thermocouples, this provides a single sensor with both outstanding resolution and amazing sensitivity.

The two integrated heaters enable the patented electrical heat flow adjustment across the entire measurement range.

Electrical Heat Flow Adjustment for the Entire Temperature Range

For the first time in DSC history, thanks to two integrated heaters in the MMS 1 sensor, electrical heat flow adjustment is available for the entire temperature range. The heaters provide a pulse of heat every 50 K, which is very accurately measured. No samples are required and there is no operator bias.

This unique, patented feature saves valuable time and your DSC is always correctly adjusted over the entire temperature range.

Electrical Heat Flow Adjustment for the Entire Temperature Range

Heat Flux Mode

Exceptional Sensitivity for the Measurement of Weak Effects

How Does Heat Flux Mode Work in the DSC 5+?

The heat flow from the furnace to the sample is compared to the heat flow from the furnace to the reference crucible.

If a thermal effect or enthalpy change occurs in the sample, its temperature will deviate (∆T) from the reference, which follows the programmed temperature. The heat flow is precisely calculated from the measured ∆T.

Watch the short video above to see how ∆T changes during a typical DSC measurement.

136 thermocouples guarantee flat baselines and high sensitivity for measuring weak thermal effects.

Should I Choose Power Compensation or Heat Flux Mode?

For the first time in a single furnace DSC, you can easily switch between power compensation or heat flux mode, depending on your needs.

In power compensation mode, the power introduced by the sensor heaters is very precisely measured, providing excellent resolution for separating close-lying thermal effects.

The star-shaped arrangement of thermocouples means both heat flux and power compensation mode provide outstanding sensitivity for measuring weak effects.

You can select the mode, according to the needs of each experiment!

Discover more in the DSC 5+ brochure

The Revolutionary MMS 1 Sensor

A Huge Leap in DSC Technology

The revolutionary MMS 1 sensor of the DSC 5+ represents a huge leap in DSC technology.

With 136 thermocouples plus 2 integrated heaters for power compensation mode, we provide a single sensor with an extremely fast signal time constant for high resolution, and an exceptional signal-to-noise ratio for increased sensitivity.

The ceramic sensor is incredibly robust and chemically resistant. Measurements can be performed at high temperatures in aggressive atmospheres without risk of corrosion.

Layering System of the MMS 1 Sensor

Revolutionary Sensor with 136 Thermocouples

Layers 1 and 2: 136 Thermocouples (2 x 68)

The two-layer design provides unmatched sensitivity for DSC. With two layers of 68 thermocouples, the measurement signal is amplified, providing an exceptional signal-to-noise ratio.

High sensitivity
Detects very weak effects

Layer 3: Two Heaters for Power Compensation Mode

Two heaters (250 µW each) are integrated into the sensor, one under the sample and one under the reference. They are activated during measurements in power compensation mode.

Outstanding resolution
Separates overlapping effects

Layer 4: Sample and Reference Temperature Sensors

Two temperature sensors precisely measure the absolute temperature of the sample crucible and reference crucible. The MMS 1 sensor is capable of measuring temperature in the range –150 to +700 °C

Wide temperature range
Accurate measurements

Repeatable Results Regardless of the Operator

Automatic exchange of the reference crucible
Automatic return of the sample crucible to the tray
Hands-free access to the furnace
Automatic crucible disposal if needed

Automated reference crucible exchange: When the sample crucible type changes, the robot exchanges the reference crucible ensuring a flat baseline for your measurements without the need for manual intervention. No more waiting around just to change the reference crucible!

Automated sample crucible exchange: The robot places the sample on the sensor and the measurement starts. After the measurement, the robot returns the sample crucible to the tray and moves on to the next experiment.

Automated crucible disposal: If required, the DSC 5+ robot disposes of the used crucible into a dedicated crucible bin. This prevents contamination of fresh samples in the crucible chamber.

Watch the video to learn about our innovative hardware and software automation solutions.

Unrivalled Modular Concept

With Full Modularity
Upgrade at Any Time
Satisfy Current and Future Needs

1. Basic, Simple and Elegant

Operate the DSC 5+ module from a PC running the STARe software, and easily manage the furnace lid when manually placing or removing crucibles. An elegant and uncomplicated solution for your workspace.

2. Interactive Touch Screen

If your DSC is not close to the PC, add the intuitive touch screen to easily control the module and monitor your experiments. Use the OneClick™ functionality to quickly start predefined methods. Simply select the method, add the sample details, and you are ready to measure.

3. Hands-Free Furnace Lid

The automatic furnace lid is simple to use and removes the risk of contamination due to manual handling. The lid is always placed correctly on the furnace, meaning measurement conditions are reproduceable and user safety is ensured.

4. Complete Robot Automation

The 3-axis sample robot, allows you to perform more experiments, in a shorter time, with less resources. With automatic reference handling, lid piercing, and crucible disposal features, the sample robot is capable of completely automating your measurements.

5. Sustainable Cooling

The CombiCooler connects to both liquid nitrogen and the intracooler, which gives you maximum flexibility. To reduce consumption, the instrument will automatically select the correct cooling for the method, using liquid nitrogen only when required by the measurement conditions.

Equip Your DSC 5+ with STARe, the Most Comprehensive Thermal Analysis Software on the Market

Unlimited evaluation possibilities
Time-saving automation options
Tailor-made, modular solutions
Unrivalled flexibility

Download the STARe Software Brochure

Download the brochure to discover the most complete and comprehensive thermal analysis software on the market.

Ready To Boost Your Lab Efficiency And Completely Automate Your Measurements?

Reach Out For a Live Demo, Additional Documentation or Any Other Requests

MultiStar™ sensor with 136 thermocouples

Exceptional sensitivity for the measurement of weak effects.

Power compensation

Provides outstanding resolution for separating close-lying effects.

Patented electrical heat flow adjustment

Saves time and ensures excellent measurement accuracy.

FlexMode™ technology

choose power compensation or heat flux mode for optimal DSC performance

Time-saving FlexCal™ adjustment

Guarantees accurate results under all measurement conditions.

Unrivalled modular concept

Tailor-made solutions for current and future needs.

Wide temperature range

From -150 to 700 °C in one measurement.

Robot with gas-purged sample chamber

The optional sample robot protects samples from the environment and operates reliably around the clock.

CombiCooler

This option is a combined LN2 cooling and intracooler for accessing the entire temperature range with reduced liquid nitrogen consumption.

Specifications - Thermal Analysis System DSC 5+

Temperature Range	-150 °C – 700 °C
Temperature accuracy (±)	+/-0.2 K
Signal Time Constant	0.7 s
Indium peak (height to width)	25
Cooling rate	0.001 to 50 K/min
TAWN resolution	4
TAWN sensitivity	66
Technique	Differential Scanning Calorimetry (DSC)
Sensor Output	Heat Flow
Data Sampling	Max. 50 data pts/sec
Applications	Crystallization Glass Transition Heat Capacity (cp) Kinetics Oxidation Induction Time (OIT) Temperature Modulated DSC
Sensor Types	MMS 1
Temperature precision (+/-)	0.02 K
Heating Rate	0.001 to 200 K/min

Product Brochures

Brochure: The DSC 5+ sets the new standard in differential scanning calorimetry.

Brochure: DSC 5+ Differential Scanning Calorimeter

With a choice of power compensation or heat flux mode, the DSC 5+ sets the new standard, delivering a superior performing and more productive DSC.

Brochure: STARe Excellence Software

Thermal analysis is a well-established analytical method that is widely used in many different fields. It provides laboratories with valuable results...

Brochure: The Future of Thermal Analysis

Thermal Analysis comprises a group of techniques that measure the physical or chemical properties of a sample as a function of temperature or time whi...

Brochure: Crucibles for Thermal Analysis

Crucibles serve as containers for samples during DSC and TGA measurements. They guarantee that the sensor is not contaminated during the measurement.

Datasheets

Datasheet: DSC Evaluation

This software option reduces unnecessary measurement time and improves safety when measuring unknown samples. It enables the instrument to terminate a...

AIWizard™, artificial intelligence for autonomous thermal analysis evaluations

AIWizard – Artificial Intelligence for Thermal Analysis

AIWizard™ is a revolutionary artificial intelligence (AI) solution for thermal analysis result evaluation and event identification.

Datasheet: Specific Heat Evaluation

The specific heat capacity cp is an important material property often used in calculations of thermal processes in the chemical industry. It describes...

Datasheet: STARe Software Option Quality Control

The Quality Control software option allows the user to easily control and track the quality of their product. It starts with the measurement; this ca...

Datasheet: Multiple Reference Libraries

The reference library option allows you to organize and store any type of sample information – be it your own past measurements or information acquir...

Get more efficient workflows with our advanced DSC automation features.

Differential Scanning Calorimetry Sample Robot

Discover advanced DSC automation. Achieve more with less effort when you combine the sample robot with the unique automation features of STARe softwar...

Know-how

Thermal Analysis of Polymers – Applications Handbook

Thermal Analysis of Polymers – Selected Applications

Find applications on the most important thermal techniques for characterizing thermoplastics, thermosets, and elastomers: DSC, TGA, TMA, and DMA.

Thermal Analysis Tips and Hints Guide

Our TA Tips and Hints Guide is designed to help you navigate through the different measurement techniques, method parameters, and sample preparation p...

Guide: Thermal Analysis for Environmental Industries

Thermal Analysis for Environmental Industries – Selected Applications

Find useful applications on important thermal techniques for renewable energy, batteries, phase change materials, biopolymers, and recycling.

Thermal Analysis of Lithium-Ion Batteries

A practical guide for the characterization of lithium-ion batteries by thermal analysis.

Materials Failure Analysis

Identify the physical roots of failures using a suite of powerful thermal analysis solutions.

Thermal Analysis Options and Accessories

Crucible Sealing Press

Material No.: 119410

Alumina Crucibles for Thermal Analysis

Crucible 30 uL, Alox, 20 pcs

Aluminum oxide crucibles

Material No.: 51140843

Aluminum Crucibles for Thermal Analysis

Crucible 40 uL, Al, 100 pcs

Aluminum Crucibles

Material No.: 26763

Pan 40 uL, Al, 400 pcs

Aluminum Crucibles

Material No.: 51119870

Crucible Light, 20 uL, Al, 100 pcs

Aluminum Crucibles

Material No.: 51119810

Pan 100 uL, Al, 400 pcs

Aluminum Crucibles

Material No.: 51119872

Gold Crucibles for Thermal Analysis

Crucible 40 uL, Au, 6 pcs

Set of 6 gold crucibles with lids. The gold pan is chemically resistant. Other than some types of aluminum pans, it is the only pan that can be hermetically sealed by cold welding. The maximum permitted pressure is 0.25 MPa.

Material No.: 27220

High Pressure Crucibles for Thermal Analysis

Crucible HP 40 uL, SST/Au, 25 pcs

Set of 25 crucibles (without pin), lids and rupture disks. The gold-plated steel crucibles have proven highly effective in the field of safety investigations. They can only be used for one measurement each. The maximum pressure is 15 MPa.

Material No.: 26731

Platinum Crucibles for Thermal Analysis

Crucible 30 uL, Pt, 4 pcs

Platinum Crucibles

Material No.: 51140842

Search suggestions

DSC 5+ The Next Generation of Performance

The revolutionary DSC 5+ comes paired with the new MMS 1, which has 136 thermocouples and 2 integrated heaters for power compensation mode and provides superior performance

Experience the Future of DSC Automation in Under 3 Minutes

More Experiments, in a Shorter Time, with Less Resources

‍High Sample Throughput with Advanced Hardware and Software Solutions

‍High Sample Throughput with Advanced Hardware and Software Solutions

The gas-controlled crucible chamber holds 96 sample and 7 reference crucibles for continuous measurement

Let the DSC 5+ Sample Robot Take the Effort Out of Your Work

Unique System of Robot Lid Piercing and Removal For Sensitive Samples

Unique System of Robot Lid Piercing and Removal For Sensitive Samples

Protect Even the Most Sensitive Samples

Download the DSC 5+ Brochure

Unique Power Compensation Mode

Unique Power Compensation Mode

Outstanding Resolution for the Separation of Close-Lying Effects

How Does Power Compensation Mode Work in the DSC 5+?

What Are the Benefits of Power Compensation Mode in the DSC 5+?

Electrical Heat Flow Adjustment for the Entire Temperature Range

Heat Flux Mode

Heat Flux Mode

Exceptional Sensitivity for the Measurement of Weak Effects

How Does Heat Flux Mode Work in the DSC 5+?

Should I Choose Power Compensation or Heat Flux Mode?

The Revolutionary MMS 1 Sensor

The Revolutionary MMS 1 Sensor

A Huge Leap in DSC Technology

136 Thermocouples Plus 2 Integrated Heaters

Layering System of the MMS 1 Sensor

Layers 1 and 2: 136 Thermocouples (2 x 68)

Layer 3: Two Heaters for Power Compensation Mode

Layer 4: Sample and Reference Temperature Sensors

Repeatable Results Regardless of the Operator

Repeatable Results Regardless of the Operator

Boost Lab Efficiency with Fully Automated Crucible Handling

Transform Your Lab with Our Exciting DSC 5+ Automation Solutions

Unrivalled Modular Concept

Unrivalled Modular Concept

Customize Your DSC 5+ at Any Time

1. Basic, Simple and Elegant

2. Interactive Touch Screen

3. Hands-Free Furnace Lid

4. Complete Robot Automation

5. Sustainable Cooling

Equip Your DSC 5+ with STARe, the Most Comprehensive Thermal Analysis Software on the Market

Equip Your DSC 5+ with STARe, the Most Comprehensive Thermal Analysis Software on the Market

Download the STARe Software Brochure

Ready To Boost Your Lab Efficiency And Completely Automate Your Measurements?

Ready To Boost Your Lab Efficiency And Completely Automate Your Measurements?

Reach Out For a Live Demo, Additional Documentation or Any Other Requests

MultiStar™ sensor with 136 thermocouples

Power compensation

Patented electrical heat flow adjustment

FlexMode™ technology

Time-saving FlexCal™ adjustment

Unrivalled modular concept

Wide temperature range

Robot with gas-purged sample chamber

CombiCooler

Specifications

Specifications - Thermal Analysis System DSC 5+

Documentation

Product Brochures

Datasheets

Know-how

Accessories

Thermal Analysis Options and Accessories

Consumables

Alumina Crucibles for Thermal Analysis

Aluminum Crucibles for Thermal Analysis

Gold Crucibles for Thermal Analysis

High Pressure Crucibles for Thermal Analysis

Platinum Crucibles for Thermal Analysis

Software

More Information

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DSC 5+

The Next Generation of Performance