Heat Flow Calorimeter - Calorimetry

EasyMax 102 HFCal

Heat Flow Calorimetry for Process Safety Screening

A small scale reaction calorimeter designed for process safety screening, EasyMax HFCal (Heat Flow Calorimeter) provides reaction information early in the development process to improve the chemical workflow.  This data can be used to characterize, optimize and understand process parameters in a controlled, accurate and reproducible environment.

EasyMax 102 HFCal reaction calorimetry workstation provides thermodynamic information including:

  • Heat Transfer Coefficient
  • Specific Heat of Reaction Mass
  • Reaction Enthalpy
  • Heat of Reaction under both isothermal and non-isothermal conditions
  • Thermal Conversion
  • Adiabatic Temperature Rise

Independent of the scale, the EasyMax 102 HFCal calorimetric screening tool provides the true heat release pattern under both isothermal and non-isothermal conditions. EasyMax 102 HFCal identifies scalability issues and eliminates potentially unfeasible routes earlier – saving time, materials and costs.  This heat flow calorimeter allows chemistry decisions to be taken sooner enabling faster process development and safer scale-up.

iControl software determines heat flow, enthalpy, heat transfer and specific heat to understand reaction parameters and uncover potential safety issues. 

EasyMax 102 HFCal is available as an all inclusive Starter Kit (30090574) or by upgrading any existing EasyMax 102 Advanced reactor system with the Upgrade Kit EasyMax HFCal (30090576).

Heat Flow Calorimetry for Process Safety Screening
Specifications - EasyMax 102 HFCal
Dimensions (WxDxH) 120 mm x 40 mm x 170 mm
Precision Heat Transfer Typically +/- 4%
Accuracy and Precision Specific Heat Typically +/- 12%
Accurate Heat Flow Isothermal conditions: ± 3% to 5%;Non-isothermal conditions: ± 5% to 10%;Based on a comparison of qr_hf with qc resp. ∫qr_hf with ∫ qc
Calorimetry Type Heat Flow
Material Number(s) 30090576

Documentation

Product Brochures

Datasheets

HFCal Heat Flow Calorimetry (US/Letter)
Heat flow calorimetry workstations provide heat release data, reaction enthalpy and heat transfer as well as heat data enabling chemistry and process...
HFCal (A4)
Heat flow calorimetry workstations provide heat release data, reaction enthalpy and heat transfer as well as heat data enabling chemistry and process...
iControl Data Sheet
iControl provides the tools to facilitate a comprehensive understanding of the chemical reaction under study. The combination of reactor data with inf...
iControl Software (A4)
iControl provides the tools to facilitate a comprehensive understanding of the chemical reaction under study. The combination of reactor data with inf...

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Software

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Capture, Prepare, Share Experimental Data

Applications

Chemical Process Safety
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EasyMax 102 HFCal

Accessories

Heat Flow Calorimeter Accessories

Chemical Synthesis Reactors

The Dosing Unit DU SP-50 allows unattended dosing combined with safe control of the reaction temperature in conjunction with the EasyMax and OptiMax synthesis reactor systems.
Hydrogenation, chlorination, carboxylation, carbonylation reactions are frequently used reactions in which the consumption of gas is a key parameter. Also understanding mass transfer in gas/liquid reactions assumes thorough understanding of the gas uptake profiles. The gas uptake sets - either fully automated or manual - in combination with iControl Software are easy to use, provide all necessary information and available for different pressure ranges.
The 100 mL sized two-piece reactor is designed to not just to hold temperature probes and pH, but also process analytical probes.
The 100 mL High Workup Volume 2-Piece Glass Reactor offers the option to add another 100 mL of liquid to quench or workup the reaction mass with the same vessel.
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EasyMax 102 HFCal
 
 
 
 
 
 
 
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