Recrystallization Guide: Process, Procedure, Solvents

Recrystallization

Optimization of Crystal Properties and Process Performance

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7 Steps of Recrystallization

Recrystallization Thermodynamics and Kinetics

Solid/Liquid Separation for Recrystallization
Drying Recrystallization
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Publications

White Papers

How to Optimize a Crystallization Step Using Simple Image Analysis
By quickly identifying unnecessary hold times and determining how cooling rate influences crystal growth and nucleation, the cycle time for an interme...
Understand Crystallization with In-Situ Microscopy
Dynamic mechanisms key to understanding crystallization processes can now be observed with in-situ microscopy. A white paper explains how leading chem...
Crystallization Process pdf
This white paper introduces you to the fundamentals of crystallization process development and provides guidance for the design of a high quality crys...
crystal size distribution ppt
This white paper discusses strategies to optimize crystal size distribution during process development and manufacturing.
industrial crystallization white paper
Optimization of the industrial crystallization process leads to increased yield and purity, reduced energy consumption and cost, and improved product...
seeding crystallization process
Seeding is a key step in optimizing a crystallization process, ensuring a consistent filtration rate, yield, polymorphic form and particle size distri...
Scale-up of Batch Crystallization From Lab to Plant
Scale-up of crystallization is notoriously complicated and companies are under pressure to develop scalable crystallization processes faster - at lowe...
Best Practices for Crystallization Development
This white paper demonstrates the methodology chemists use to optimize critical crystallization parameters such as temperature profile, addition rates...
Particle Characterization From Small Scale Lab Reactors to Full Scale Production Pipelines
Particle size analysis approaches are deployed for effective delivery of high quality particle products. Combining offline particle size analyzers wi...

Webinars

Continuous Flow Chemistry Using PAT
Eric Fang of Snapdragon discusses how continuous flow chemistry is applicable across the entire value chain. Early implementation of continuous flow...
Eliminating Micronization Using Fine Particle Crystallization
Crystal engineering is applied when the crystal size distribution is too large to meet downstream specifications. By designing the crystallization to...
Calibration Free Supersaturation Assessment
The quantitative use of in situ ATR-FTIR for real time supersaturation assessment has been extremely well defined within the literature. However, thes...
metastable zone width (MSZW) crystallization
The webinar focuses on a semi-quantitative method for the optimization and scale-up of hydrodynamically limited anti-solvent crystallization process....
Improving Crystallization and Precipitation
This webinar introduces case studies and highlights best practices used to overcome crystallization and precipitation challenges. The focus will be on...
Improving Crystallization and Precipitation
This webinar introduces case studies and highlights best practices used to overcome crystallization and precipitation challenges. The focus will be on...
Liquid-Liquid Phase Separation in Crystallization
Design and develop robust, scalable crystallization processes that avoids Liquid-Liquid Phase Separation (LLPS) or oiling out.
Improving Crystallization and Precipitation
This webinar introduces case studies and highlights best practices used to overcome crystallization and precipitation challenges. The focus will be on...
Crystallization Scale-up Strategy Development
During this webinar, two case studies are presented to illustrate the application of tools and strategies that were utilized to understand and manage...
Wet Milling Impact on Particle Size
This presentation details the development, understanding, and scale-up of an aseptic crystallization, which utilizes a novel wet milling during anti-s...
Pharmaceutical Drug Substance Crystallization
This presentation describes the case of crystals of an Active Pharmaceutical Ingredient (API) with high propensity to float in their mother liquors, d...
Automated Alternative to Manual Solution Sampling in Solid-Liquid Systems
In this talk, the application of EasyFrit — an automated alternative to manual solution sampling in solid-liquid systems — is presented for pharmaceut...

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