Phase Correction in ADSC

In ADSC measurements, the raw data of phase angle shows a deviation from the theoretical value of zero before and after the phase transition. This is caused by the heat transfer between the instrument and the sample and within the sample itself. This article presents a scientifically acceptable correction procedure of the phase angle.

 

 

 

 

 

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Keywords
UserCom 6
  20
 polycarbonate (PC), phase angle, modulated DSC, temperature modulated DSC, oscillating DSC
 


 

Phase correction in ADSC measurements in glass transition | Thermal Analysis Application No. UC 68 | Application published in METTLER TOLEDO Thermal Analysis UserCom 6