Uncovering Scale-up and Safety Issues
OptiMax HFCal is a reaction calorimeter that generates calorimetric information under both isothermal as well as non-isothermal conditions. The system is Plug & Play and ready to run any desiged unit operation automatically - or manually if preferred.
Heat Flow Calorimetry – Simple and Accurate
OptiMax HFCal reproducibly delivers information to characterize and scale-up processes ensuring they are safe at scale.
At the push of a button, iControl software automatically calculates heat data, including:
- Heat transfer coefficient
- Specific heat of the reaction mass
- Heat flow for isothermal and non-isothermal conditions
- Thermal conversion
- Adiabatic temperature rise
iControl Software creates a report including trends and tables of experimental results.
Heating and Cooling – No Additional Cryostat Needed
Heating and cooling is fast and does not require a cryostat. The electrical heating and Peltier cooling ensure precise temperature control from -40 °C to 180 °C.
All events and data are recorded automatically, making experiments traceable and reproducible. At the end of the experiment, the relevant data is summarized and a report with tables and trends is generated automatically. For further processing, interpretation or storage purposes, iC Data Center or the Microsoft® Excel® can be used.
|Dimensions (WxDxH) Dimensions (WxDxH):120 mm x 40 mm x 170 mm||120 mm x 40 mm x 170 mm|
|Precision Heat Transfer Precision Heat Transfer:Typically +/- 3%||Typically +/- 3%|
|Accuracy and Precision Specific Heat Accuracy and Precision Specific Heat:Typically +/-10%||Typically +/-10%|
|Accuracy Heat Flow Accuracy Heat Flow:Isothermal conditions: ± 3 % to 5 %Accuracy Heat Flow:Non-isothermal conditions: ± 5 % to 10%Accuracy Heat Flow:Based on comparison of qr_hf with qc resp. ∫qr_hf with ∫ qc||Isothermal conditions: ± 3 % to 5 %; Non-isothermal conditions: ± 5 % to 10%; Based on comparison of qr_hf with qc resp. ∫qr_hf with ∫ qc|
|Calorimetry Type Calorimetry Type:Heat Flow||Heat Flow|
|Cooling Performance||0°C 35 W |
20°C 65 W
40°C 95 W
|Temperature Range||-40°C to 180°C (jacket temperature)|
|Control Modes||isothermal and isoperibolic, constant or ramp, reflux, distillation & crystallization|
|Stirring||30 rpm to 1200 rpm|
|Dimensions||Thermostat: 388 mm x 414 mm x 539 mm|
|Power Supply||100 V to 240 V AC, 50 Hz to 60 Hz, 1300 VA|
|Operation||iControl software for calorimetric applications|
Graphical touchscreen and/or iControl Software
|Type||Single piece or two piece (with bottom drain valve)|
|Pressure||50 mbar to 1 bar|
|Stirrer||Pitch-blade (glass, Alloy 22)|
Anchor (glass, Alloy 22)
Half-moon (PTFE for single piece reactor)
|Calibration Heater||Max. 20 W|
|Precision Heat Transfer||Typically ± 3%|
|Accuracy and Precision Specific Heat||Typically ± 10%|
|Accuracy Heat Flow||Typically ± 3% to 5%, under isothermal conditions|
Typically ± 5% to 10%, under non-isothermal conditions
|Sensitivity||≤0.1 W measured as standard deviation of qr under steady state conditions.|
Peak-to-peak noise is ≤ approximately 0.4 W.
|Power and Data Interface||Direct connection to CAN interface of standard OptiMax,|
no additional power supply or PC connection required
|Data Logging||Via iControl Software|
|Dimensions||120 mm x 40 mm x 170 mm|
|Software||iControl 5.2 or higher required, HFCal license|