High Pressure Reactions - METTLER TOLEDO

High Pressure Reactions

Understand and Characterize High Pressure Reactions Under Challenging Sampling Conditions

Many processes require reactions to be run under high pressure. Working under pressure is challenging and collecting samples for offline analysis is difficult and time consuming. A change in pressure could affect reaction rate, conversion and mechanism as well as other process parameters plus sensitivity to oxygen, water, and associated safety issues are common problems.



Utilizing in situ reaction analysis (ReactIR) under pressure enables the tracking of reaction progression, determination of reaction kinetics, pathway and mechanism and the qualitative and quantitative detection of reaction components. The information gained from ReactIR can be used to determine critical process parameters, improve process efficiency and robustness and produce consistent product quality. 

Synthesis workstations (EasyMax) enable high pressure process characterization and the development of robust chemical processes at scale. EasyMax evaluates reaction parameters such as gas consumption, mass transfer, kinetic activity and heterogenic catalysis in mid and high-pressure reactions.

Gas consumption is a key parameter in hydrogenation, chlorination, carboxylation and carbonylation reactions. Understanding gas consumption as well as mass transfer in gas/liquid reactions requires an in-depth understanding of gas uptake profiles.

The iC software suite allows scientists and engineers to convert experiment data into important process knowledge - providing critical information to make better decisions, and therefore complete projects faster. The seamless integration of complementary data sets (spectroscopy, reactor control, particle characterization) further supports the faster understanding of the process under investigation.

Applikationen

Applikationen

Nitrobenzyl reduction
Gain insights into difficult chemistryGain insights into reaction performance and variableswhen conditions prohibit or complicate extractive sampling...

Publikationen

On-Demand Webinars

Neues Webinar über Reaktionen unter erhöhtem Druck
Die Nachfrage nach unter erhöhtem Druck ablaufenden Reaktionen steigt. In der Druckchemie besteht die Reaktionsmasse in der Regel aus mehreren Phasen,...
Hydrogenation Under High Pressure
Diese Präsentation diksutiert die Implementierung der Fourier-Transformations-Infrarot (FTIR)-Reaktionskontrolltechnologie, um Wissen und ein Verständ...

White Papers

Überwachung chemischer Reaktionen in kürzerer Zeit
„Wie kann mit geringerem Aufwand mehr erreicht werden“ – dies ist eine in chemischen Entwicklungslabors ständig gestellte Frage, da Forscher chemische...

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